O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

Base Information

Chemical Name:O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate
CAS No.:1225012-22-5
Molecular Formula:C₂₃H₂₄NOPS
Molecular Weight:393.489
Hs Code.:

Synonyms:O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

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Chemical Property of O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

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Technology Process of O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

There total 2 articles about O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1225012-18-9
3-(diphenylthiophosphoryl)oxybenzaldehyde

: 75-64-9
tert-butylamine

: 1225012-22-5
O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 54h;
DOI:10.1021/om9009894

Reference yield:

: 1015-37-8
diphenylthiophosphinoyl chloride

: 100-83-4
meta-hydroxybenzaldehyde

: 75-64-9
tert-butylamine

: 1225012-22-5
O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

Guidance literature:: diphenylthiophosphinoyl chloride; meta-hydroxybenzaldehyde; With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; benzene;

tert-butylamine; With magnesium sulfate; In water; benzene;
DOI:10.1080/10426507.2010.507726

Reference yield: 53.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 1225012-22-5
O-[3-[(tert-butylimino)methyl]phenyl] diphenylthiophosphinate

: 1225012-26-9
[2-[(diphenylthiophosphoryl)oxy]-6-[(tert-butylimino)methyl]phenyl]palladium chloride

Guidance literature:: In benzene; soln. of Pd complex in C6H6 was slowly dropwise added to soln. of ligandin C6H6; refluxed with stirring for 2 h; cooled to room temp.; filtered; evapd.; recrystd. (CH2Cl2/Et2O, 1/2); elem. anal.;
DOI:10.1021/om9009894