(1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione

Base Information

• Chemical Name: (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione
• CAS No.: 122093-00-9
• Molecular Formula: C₁₇H₁₈NO₄PS
• Molecular Weight: 363.374

Synonyms:(1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione

Chemical Property of (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione

There total 1 articles about (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ⁵-phospha-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

endo-3-ethoxy-6-methyl-N-phenyl-2,3-oxaphosphabicyclo<2.2.2>oct-5-ene-8,9-dicarboxamide 3-oxide (96326-62-4,131724-80-6) → (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ5-phospha-tricyclo[5.2.2.02,6]undec-10-ene-3,5-dione (122093-00-9)

Guidance literature:

With tetraphosphorus decasulfide; In dichloromethane; for 144h; Ambient temperature;

DOI:10.1021/ja00199a061

Reference yield:

(1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ5-phospha-tricyclo[5.2.2.02,6]undec-10-ene-3,5-dione (122093-00-9) + tert-butyl alcohol (75-65-0) → N-phenyl-4-methyl-1,2-dihydrophthalimide (75581-74-7) + Thiophosphoric acid O-tert-butyl ester O'-ethyl ester (55882-48-9)

Guidance literature:

With triethylamine; In toluene; at 110 ℃; for 2h;

DOI:10.1021/ja00199a061

Reference yield:

ethanol (64-17-5) + (1S,2R,6R,7S)-9-Ethoxy-11-methyl-4-phenyl-9-thioxo-8-oxa-4-aza-9λ5-phospha-tricyclo[5.2.2.02,6]undec-10-ene-3,5-dione (122093-00-9) → N-phenyl-4-methyl-1,2-dihydrophthalimide (75581-74-7) + O,O'-diethyl thiophosphoric acid (2465-65-8)

Guidance literature:

In toluene; at 110 ℃; for 2h;

DOI:10.1021/ja00199a061

upstream raw materials:

endo-3-ethoxy-6-methyl-N-phenyl-2,3-oxaphosphabicyclo<2.2.2>oct-5-ene-8,9-dicarboxamide 3-oxide

Downstream raw materials:

N-phenyl-4-methyl-1,2-dihydrophthalimide

O,O'-diethyl thiophosphoric acid

thiophosphoric acid O-ethyl ester O'-isopropyl ester

Thiophosphoric acid O-tert-butyl ester O'-ethyl ester

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