zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

Base Information

Chemical Name:zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))
CAS No.:126581-06-4
Molecular Formula:C₄₄H₁₉Cl₈N₅O₂Zn
Molecular Weight:998.681
Hs Code.:

zinc(NO<sub>2</sub>)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

Synonyms:zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

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Technology Process of zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

There total 2 articles about zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 100506-72-7
[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato] zinc(II)

: 7697-37-2,78989-43-2
nitric acid

: 126581-06-4
zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

Guidance literature:: With CF₃SO₃H; (CF₃SO₂)2O; In dichloromethane; treated with HNO3-CF3SO3H-(CF3SO2)2O (1:0.12:0.06)(1.1 equivalent of HNO3) at 20°C for 24 h; elem. anal., UV, NMR, MAS;
DOI:10.1039/b004160m

Reference yield: 71.0%

: 100506-72-7
[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato] zinc(II)

: 10102-44-0
Nitrogen dioxide

: 126581-06-4
zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

Guidance literature:: In dichloromethane; gaseous nitrogen dioxide is added to a soln. of Zn(OCP) in CH2Cl2, stirring for 2 h at room temp.; soln. is reduced to dryness, chromd. on alumina (1/1 CH2Cl2/toluene, 1/2 Ch2Cl2/toluene), addn. of cyclohexane to eluent;

Reference yield: 71.0%

: 126581-06-4
zinc(NO₂)(meso-(tetrakis(2,6-dichlororophenyl)porphine))

: 2-nitro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrin

Guidance literature:: In trifluoroacetic acid; demetallation of Zn(NOCP) by treatment with trifluoracetic acid for 1 h; workup with ammonium hydroxide, crystn. (CH2Cl2/heptane); elem. anal., UV-vis, (1)H-NMR;