N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

Base Information

Chemical Name:N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine
CAS No.:1338685-19-0
Molecular Formula:C₂₂H₃₁ClN₂O
Molecular Weight:374.954
Hs Code.:

N<sub>1</sub>-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

Synonyms:N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

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Technology Process of N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

There total 9 articles about N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63649-64-9
4-isopropyl-2-nitrobenzenamine

: 1338685-19-0
N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 2 h / 760.05 Torr

With hydrogen; sodium hydride; In ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1338685-18-9
N-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropyl-2-nitroaniline

: 1338685-19-0
N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

Guidance literature:: With hydrogen; In ethanol; for 2h; under 760.051 Torr;

Reference yield:

: 1338685-13-4
isobutyl 3-(4-chlorophenyl)-2-isobutoxyacrylate

: 1338685-19-0
N₁-[3-(4-chlorophenyl)-2-isobutoxypropyl]-4-isopropylbenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen; zinc dibromide / palladium 10% on activated carbon / ethyl acetate / 42 h / 20 °C / 760.05 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C

3.1: triphenylphosphine; bromine / dichloromethane / 24.5 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

4.2: 18 h / 20 °C

5.1: hydrogen / ethanol / 2 h / 760.05 Torr

With lithium aluminium tetrahydride; hydrogen; bromine; sodium hydride; triphenylphosphine; zinc dibromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;