(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Base Information

Chemical Name:(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone
CAS No.:82933-46-8
Molecular Formula:C₁₇H₁₇N₃O₄S
Molecular Weight:359.406
Hs Code.:

Synonyms:(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Suppliers and Price of (3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

There total 7 articles about (3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 82933-47-9
Methanesulfonic acid (1R,2S)-2-benzyloxycarbamoyl-1-methyl-2-(2-nitro-phenylsulfanylamino)-ethyl ester

: 82933-48-0
(3S,4R)-3-<<(o-nitrophenyl)sulfenyl>amino>-4-methyl-2-oxetanone

: 82933-46-8
(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Guidance literature:: With potassium carbonate; In acetone; for 3h; Heating;
DOI:10.1021/ja00386a035

Reference yield:

: N₂-[(2-nitrophenyl)thio]-N-(phenylmethoxy)-L-threoninamide

: 124-63-0
methanesulfonyl chloride

: 82933-46-8
(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Guidance literature:: With potassium carbonate; In pyridine; acetone;

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 82933-46-8
(3S-trans)-4-Methyl-3-[[(2-nitrophenyl)thio]amino]-1-(phenylmethoxy)-2-azetidinone

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1.) 0-5 deg C, 30 min, 2.) 26 deg C, 12 h

2: 9.6 g / pyridine / 2 h / 0 °C

3: 24 percent / anhydrous potassium carbonate / acetone / 3 h / Heating

With pyridine; potassium carbonate; In dichloromethane; acetone;
DOI:10.1021/ja00386a035