triethylaluminum*THF

Base Information

• Chemical Name: triethylaluminum*THF
• CAS No.: 856321-23-8
• Molecular Formula: C₄H₈O*C₆H₁₅Al
• Molecular Weight: 186.274
• Mol file: 856321-23-8.mol

Synonyms:triethylaluminum*THF

Chemical Property of triethylaluminum*THF

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of triethylaluminum*THF

There total 1 articles about triethylaluminum*THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + diethylmagnesium (557-18-6) + ethylaluminum dichloride (563-43-9) → triethylaluminum*THF (856321-23-8) + diethylaluminum chloride*THF (859747-71-0) + Mg2Cl3(1+) + Li(1+)*(C2H5)2AlCl2(1-)=LiAlCl2(C2H5)2 + magnesium chloride (7786-30-3)

Guidance literature:

In tetrahydrofuran; hexane soln. of EtAlCl2 vac. dried, THF added, stirred for 30 min, Et2Mgin THF added dropwise; detd. by Raman spectra;

DOI:10.1021/om061076s

Reference yield:

(C2H5)3Al*tetrahydrofuran (856321-23-8) + tin(ll) chloride → tetraethyltin (597-64-8)

Guidance literature:

under Ar at 90°C;

upstream raw materials:

tetrahydrofuran

diethylmagnesium

ethylaluminum dichloride

Downstream raw materials:

tetraethyltin