Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI)
CAS No.:119908-77-9
Molecular Formula:C₇H₉ClO₃
Molecular Weight:176.6
Hs Code.:
Mol file:119908-77-9.mol

Synonyms:Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI)

Chemical Property:

PSA：54.37000
LogP:1.25270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI)

There total 2 articles about Cyclopropanecarboxylic acid, 2-(chlorocarbonyl)-1,2-dimethyl-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6914-70-1
1,2-Dimethyl-r-1,c-2-cyclopropandicarbonsaeure-dimethylester

: 119908-77-9
c-2-Chlorformyl-1,2-dimethyl-r-1-cyclopropancarbonsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KOH; 2.) HCl / 1.) CH₃OH, 2 h; 2.) THF, H₂O, -10 to 0 deg C

2: PCl₅ / 1.5 h

With hydrogenchloride; potassium hydroxide; phosphorus pentachloride;

Reference yield:

: 699-49-0
cis-1,2-Dimethyl-1,2-cyclopropanedicarboxylic acid

: 6914-67-6
1,2-dimethyl-cyclopropane-1r,2c-dicarboxylic acid anhydride

: 119908-77-9
c-2-Chlorformyl-1,2-dimethyl-r-1-cyclopropancarbonsaeure

: 119908-74-6
(1R,2S)-1,2-Dimethyl-cyclopropane-1,2-dicarbonyl dichloride

Guidance literature:: With phosphorus pentachloride; for 1.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;