CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER

Base Information

• Chemical Name: CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER
• CAS No.: 6914-70-1
• Molecular Formula: C9H14O4
• Molecular Weight: 186.20506
• Hs Code.: 2917209090
• Mol file: 6914-70-1.mol

Synonyms:CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER;1,2-DIMETHYL-1,2-DIMETHYL CYCLOPROPANE DICARBOXYLATE;cis-1,2-Dimethylcyclopropanedicarboxylicaciddimer

Chemical Property of CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER

Chemical Property:

• Boiling Point: 114-116 °C(Press: 23 Torr)
• PSA: 52.60000
• Density: 1.126±0.06 g/cm3(Predicted)
• LogP: 0.74870

Purity/Quality:

98% ^*data from raw suppliers

CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER

There total 12 articles about CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

2-chloro-propionic acid methyl ester (17639-93-9) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → 1,2-Dimethyl-r-1,t-2-cyclopropandicarbonsaeure-dimethylester (6914-83-6) + 1,2-Dimethyl-r-1,c-2-cyclopropandicarbonsaeure-dimethylester (6914-70-1)

Guidance literature:

With methanol; sodium hydride; In N,N-dimethyl-formamide; paraffin; at 50 - 70 ℃; for 12h;

Reference yield:

Dimethyl meso-2,4-dibromo-2,4-dimethylglutarate → 1,2-Dimethyl-r-1,t-2-cyclopropandicarbonsaeure-dimethylester (6914-83-6) + 1,2-Dimethyl-r-1,c-2-cyclopropandicarbonsaeure-dimethylester (6914-70-1)

Guidance literature:

With (PPh₃)2N⁽¹⁺⁾*Cr(CO)4NO^(1-); In dichloromethane; at -78 ℃; Yield given. Yields of byproduct given;

Reference yield:

2-chloropropyl methyl ester (817-76-5) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → 1,2-Dimethyl-r-1,c-2-cyclopropandicarbonsaeure-dimethylester (6914-70-1)

Guidance literature:

With sodium hydride; In toluene;

DOI:10.1021/jo01082a002

upstream raw materials:

2-chloropropyl methyl ester

methacrylic acid methyl ester

diazomethane

cis-1,2-Dimethyl-1,2-cyclopropanedicarboxylic acid

Downstream raw materials:

cis-1,2-Dimethyl-1,2-cyclopropanedicarboxylic acid

1,2-dimethyl-cyclopropane-1r,2c-dicarboxylic acid anhydride

c-2-Chlorformyl-1,2-dimethyl-r-1-cyclopropancarbonsaeure

3-phenyl-1,5-dimethyl-3-azabicyclo-<3.1.0>hexane-2,4-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 6914-70-1 CIS-1,2-DIMETHYL-CYCLOPROPANEDICARBOXYLIC ACID DIMETHYL ESTER

Send

Send

Metric Ton KG G Pound L ML

Send

Send