3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

Base Information

Chemical Name:3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone
CAS No.:367953-17-1
Molecular Formula:C₂₀H₂₅N₃S
Molecular Weight:339.505
Hs Code.:

Synonyms:3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

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Technology Process of 3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

There total 1 articles about 3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 100-63-0
phenylhydrazine

: 188251-47-0
3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline

: 367953-17-1
3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

Guidance literature:: With acetic acid; In ethanol; for 0.25h; Heating;
DOI:10.1023/A:1017575718196

Reference yield:

: 367953-17-1
3-Butyryl-1-methylthio-5,6,7,8-tetrahydroisoquinoline phenylhydrazone

: 574-60-7
3-(3-Ethylindol-2-yl)-5,6,7,8-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / montmorillonite K₁₀; ZnCl₂ / microwave irradiation

2: 63 percent / Raney Ni W-2 / ethanol / 0.17 h / 20 °C

With Montmorillonite K₁₀; Raney Ni W-2; zinc(II) chloride; In ethanol; 1: Fischer reaction;
DOI:10.1023/A:1017575718196