1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

Base Information

Chemical Name:1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate
CAS No.:137685-29-1
Molecular Formula:C₂₆H₃₀Cl₂N₂O₄S
Molecular Weight:537.507
Hs Code.:

Synonyms:1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

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Chemical Property of 1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

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Technology Process of 1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

There total 3 articles about 1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 137685-29-1
1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 3,4-dimethyl-5-(2-hydroxyethyl)thiazolium iodide / ethanol / 24 h

2: dimethylformamide / 6 h / Heating

3: 1.) sodium methoxide / 1.) CH₃OH, RT, 45 min, 2.) CH₃OH, RT, overnight

With sodium methylate; 3,4-dimethyl-5-(2-hydroxyethyl)thiazolium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00101a016

Reference yield:

: 4254-20-0
4,4'-dichlorobenzoin

: 137685-29-1
1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 6 h / Heating

2: 1.) sodium methoxide / 1.) CH₃OH, RT, 45 min, 2.) CH₃OH, RT, overnight

With sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00101a016

Reference yield:

: 137685-56-4
1,1-dimethylethyl-5,6-epoxy-3-hydroxy-3-methylhexanoate

: 23187-08-8
4,5-di-(p-chlorophenyl)-Δ⁴-imidazoline-2-thione

: 137685-29-1
1,1-dimethylethyl 6-<<4,5-bis(4-chlorophenyl)-1H-imidazol-2-yl>thio>-3,5-dihydroxy-3-methylhexanoate

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1.) CH₃OH, RT, 45 min, 2.) CH₃OH, RT, overnight;
DOI:10.1021/jm00101a016