chloromethyl(p-chlorophenyl)diphenylsilane

Base Information

• Chemical Name: chloromethyl(p-chlorophenyl)diphenylsilane
• CAS No.: 128499-28-5
• Molecular Formula: C₁₉H₁₆Cl₂Si
• Molecular Weight: 343.328
• Mol file: 128499-28-5.mol

Synonyms:chloromethyl(p-chlorophenyl)diphenylsilane

Chemical Property of chloromethyl(p-chlorophenyl)diphenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of chloromethyl(p-chlorophenyl)diphenylsilane

There total 1 articles about chloromethyl(p-chlorophenyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

4-chlorophenyl lithium (14774-78-8) + chloro(chloromethyl)diphenylsilane (2632-78-2) → chloromethyl(p-chlorophenyl)diphenylsilane (128499-28-5)

Guidance literature:

In diethyl ether; hexane; at -40 - 20 ℃; for 1h;

DOI:10.1021/jo010471j

Reference yield: 29.0%

chloromethyl(p-chlorophenyl)diphenylsilane (128499-28-5) → (p-chlorophenyl)(iodomethyl)diphenylsilane (439869-08-6)

Guidance literature:

With sodium iodide; In acetonitrile; at 82 ℃; for 48h;

DOI:10.1021/jo010471j

Reference yield:

chloromethyl(p-chlorophenyl)diphenylsilane (128499-28-5) → para-chlorotoluene (106-43-4) + toluene (108-88-3,15644-74-3,16713-13-6)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; Further Variations:; Temperatures; Product distribution;

DOI:10.1021/jo010471j

upstream raw materials:

4-chlorophenyl lithium

chloro(chloromethyl)diphenylsilane

Downstream raw materials:

para-chlorotoluene

difluorodiphenylsilane

(4-Chloro-phenyl)-difluoro-phenyl-silane

toluene