methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

Base Information

Chemical Name:methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate
CAS No.:83173-69-7
Molecular Formula:C₁₉H₃₀N₄O₆S
Molecular Weight:442.536
Hs Code.:

methyl N<sup>α</sup>-(tert-butoxycarbonyl)-N<sup>ω</sup>-tosyl-L-argininate

Synonyms:methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

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Technology Process of methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

There total 1 articles about methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 13836-37-8
Boc-Arg(Tos)-OH

: 18107-18-1
diazomethyl-trimethyl-silane

: 83173-69-7
methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

Guidance literature:: In methanol; hexane; acetonitrile; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01506

Reference yield: 88.0%

: 83173-69-7
methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

: 129397-84-8
Boc-L-Arg(Tos)-ol

Guidance literature:: With sodium tetrahydroborate; acetic acid; In 1,4-dioxane; at 80 ℃;

Reference yield: 54.0%

: 83173-69-7
methyl N^α-(tert-butoxycarbonyl)-N^ω-tosyl-L-argininate

: 149625-80-9
1,5-anhydro-6-O-triisopropylsilyl-3,4-O-carbonate-2-deoxy-D-lyxo-hex-1-enopyranose

: methyl (E)-N₂-(tert-butoxycarbonyl)-Nw-((2R,5R,6R)-5-hydroxy-6-(((triisopropylsilyl)oxy)methyl)-5,6-dihydro-2H-pyran-2-yl)-Nw'-tosyl-L-argininate

Guidance literature:: With palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In dichloromethane; at 20 ℃; for 12h; stereoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01506