tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

Base Information

Chemical Name:tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane
CAS No.:211857-40-8
Molecular Formula:C₃₁H₃₉F₃O₄Si
Molecular Weight:560.729
Hs Code.:

Synonyms:tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

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Chemical Property of tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

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Technology Process of tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

There total 1 articles about tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 211857-39-5
(1S,2R,3S)-1-[4-(tert-Butyl-diphenyl-silanyloxymethyl)-phenyl]-4,4,4-trifluoro-2-hydroxymethyl-butane-1,3-diol

: 74-88-4
methyl iodide

: 211857-40-8
tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, r.t., 30 min; 2.) THF, reflux, 3 h;
DOI:10.1002/hlca.19980810515

Reference yield: 89.0%

: 211857-40-8
tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

: 211857-41-9
[4-((1S,2R,3S)-4,4,4-Trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-phenyl]-methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1002/hlca.19980810515

Reference yield:

: 211857-40-8
tert-Butyl-diphenyl-[4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-silane

: 211857-42-0
1-Bromomethyl-4-((1S,2R,3S)-4,4,4-trifluoro-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / TBAF / tetrahydrofuran / 12 h / Ambient temperature

2: 80 percent / Ph₃P, CBr₄ / tetrahydrofuran / 16 h / Ambient temperature

With carbon tetrabromide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1002/hlca.19980810515