2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

Base Information

Chemical Name:2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate
CAS No.:1426579-77-2
Molecular Formula:C₁₈H₁₇BCl₃IO₅S
Molecular Weight:589.47
Hs Code.:

Synonyms:2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

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Chemical Property of 2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

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Technology Process of 2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

There total 6 articles about 2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15945-07-0
2,4,5-trichlorobenzensulfonyl chloride

: 1245635-14-6
2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1426579-77-2
2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo302802b

Reference yield:

: 28177-54-0
2,6-diiodo-phenol

: 1426579-77-2
2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane

2: isopropylmagnesium chloride / tetrahydrofuran

3: sodium iodide; chloro-trimethyl-silane / acetonitrile

4: dichloromethane

5: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With chloro-trimethyl-silane; isopropylmagnesium chloride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo302802b

Reference yield:

: 197149-33-0
1,3-diiodo-2-(methoxymethoxy)benzene

: 1426579-77-2
2-iodo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl 2,4,5-trichlorobenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: isopropylmagnesium chloride / tetrahydrofuran

2: sodium iodide; chloro-trimethyl-silane / acetonitrile

3: dichloromethane

4: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With chloro-trimethyl-silane; isopropylmagnesium chloride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo302802b