3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

Base Information

Chemical Name:3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole
CAS No.:1383714-71-3
Molecular Formula:C₂₂H₁₉Cl₂N₃O₂
Molecular Weight:428.318
Hs Code.:

Synonyms:3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

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Chemical Property of 3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

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Technology Process of 3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

There total 6 articles about 3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 880019-21-6
N'-(2,6-dichlorobenzylidene)-4-(1H-2,5-dimethylpyrrol-1-yl)benzohydrazide

: 108-24-7
acetic anhydride

: 1383714-71-3
3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

Guidance literature:: for 4h; Reflux;
DOI:10.1007/s00044-012-0112-0

Reference yield:

: 26165-67-3
4-(2,5-dimethyl-1H-pyrrol-1-yl)benzoic acid hydrazide

: 83-38-5
2,6-dichlorobenzaldehyde

: 1383714-71-3
3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / Reflux

2: 4 h / Reflux

With acetic acid; In ethanol;
DOI:10.1007/s00044-012-0112-0

Reference yield:

: 5159-70-6
ethyl 4-(2,5-dimethyl-1H-pyrrol-1-yl)benzoate

: 1383714-71-3
3-acetyl-5-[4-(2,5-dimethylpyrrol-1-yl)phenyl]-2-(2,6-dichloro phenyl)-2,3-dihydro-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: acetic acid / ethanol / Reflux

3: 4 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1007/s00044-012-0112-0