4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

Base Information

Chemical Name:4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole
CAS No.:1370346-49-8
Molecular Formula:C₂₀H₁₈Cl₂N₆O₄S₂
Molecular Weight:541.439
Hs Code.:

Synonyms:4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

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Chemical Property of 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

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Technology Process of 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

There total 5 articles about 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1370346-40-9
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

: 38622-91-2,36635-61-7
[(p-methylphenyl)sulfonylmethyl]isonitrile

: 1370346-49-8
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

Guidance literature:: With sodium hydride; In diethyl ether; dimethyl sulfoxide; at 20 ℃;
DOI:10.1248/cpb.59.1509

Reference yield:

: 1136056-29-5
methyl 2-(N-(4-chlorophenyl)sulfamoyl)acetate

: 1370346-49-8
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; hydrazine hydrate / methanol / Reflux

2: trichlorophosphate / Reflux

3: hydrazine hydrate / butan-1-ol / Reflux

4: sodium hydride / diethyl ether; dimethyl sulfoxide / 20 °C

With pyridine; sodium hydride; hydrazine hydrate; trichlorophosphate; In methanol; diethyl ether; dimethyl sulfoxide; butan-1-ol;
DOI:10.1248/cpb.59.1509

Reference yield:

: [(Z)-2-(4-Chloro-phenyl)-ethenesulfonyl]-acetic acid

: 1370346-49-8
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-(4-(p-chlorophenyl)-1H-pyrrol-3-ylsulfonylmethyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / Reflux

2: hydrazine hydrate / butan-1-ol / Reflux

3: sodium hydride / diethyl ether; dimethyl sulfoxide / 20 °C

With sodium hydride; hydrazine hydrate; trichlorophosphate; In diethyl ether; dimethyl sulfoxide; butan-1-ol;
DOI:10.1248/cpb.59.1509