4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

Base Information

Chemical Name:4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole
CAS No.:1370346-40-9
Molecular Formula:C₁₈H₁₇Cl₂N₅O₄S₂
Molecular Weight:502.402
Hs Code.:

Synonyms:4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

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Chemical Property of 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

Chemical Property:

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Technology Process of 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

There total 4 articles about 4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1370346-34-1
2-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,3,4-oxadiazole

: 1370346-40-9
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

Guidance literature:: 2-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,3,4-oxadiazole; With hydrazine hydrate; In butan-1-ol; Reflux;

With potassium hydroxide; In butan-1-ol;
DOI:10.1248/cpb.59.1509

Reference yield:

: [(Z)-2-(4-Chloro-phenyl)-ethenesulfonyl]-acetic acid

: 1370346-40-9
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: hydrazine hydrate / butan-1-ol / Reflux

With hydrazine hydrate; trichlorophosphate; In butan-1-ol;
DOI:10.1248/cpb.59.1509

Reference yield:

: 1136056-29-5
methyl 2-(N-(4-chlorophenyl)sulfamoyl)acetate

: 1370346-40-9
4-amino-3-(p-chlorophenylaminosulfonylmethyl)-5-[Z-(p-chlorostyrylsulfonylmethyl)]-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydrazine hydrate / methanol / Reflux

2: trichlorophosphate / Reflux

3: hydrazine hydrate / butan-1-ol / Reflux

With pyridine; hydrazine hydrate; trichlorophosphate; In methanol; butan-1-ol;
DOI:10.1248/cpb.59.1509