1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

Base Information

Chemical Name:1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene
CAS No.:292858-29-8
Molecular Formula:C₄₈H₇₃IO₁₈
Molecular Weight:1065
Hs Code.:

Synonyms:1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

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Chemical Property of 1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

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Technology Process of 1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

There total 1 articles about 1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 64339-43-1
5-iodoresorcinol

: 246140-08-9
3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzylbromide

: 292858-29-8
1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; at 60 ℃; for 20h;
DOI:10.1002/1522-2675(20000705)83:7<1346::AID-HLCA1346>3.0.CO;2-3

Reference yield: 65.0%

: (M)-3,3'-diethynyl-2,2'-bis(methoxymethoxy)-1,1'-binaphthyl

: 292858-29-8
1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

: (+)-(S)-3,3'-bis{2-[3,5-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)phenyl]ethynyl}-2,2'-bis(methoxymethoxy)-1,1'-binaphthalene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 40 ℃; for 12h;
DOI:10.1002/1522-2675(20000705)83:7<1346::AID-HLCA1346>3.0.CO;2-3

Reference yield: 34.0%

: 292858-29-8
1,3-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)-5-iodobenzene

: C₅₆H₄₂O₈

: (+)-(S,S)-3,3'-(buta-1,3-diynediyl)bis(3'-{2-[3,5-bis(3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzyloxy)phenyl]ethynyl}-2,2'-bis(methoxymethoxy)-1,1'-binaphthalene)

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 40 ℃; for 4h;
DOI:10.1002/1522-2675(20000705)83:7<1346::AID-HLCA1346>3.0.CO;2-3