ethyl 6-amino-2-chloro-3-fluorobenzoate

Base Information

Chemical Name:ethyl 6-amino-2-chloro-3-fluorobenzoate
CAS No.:153500-76-6
Molecular Formula:C₉H₉ClFNO₂
Molecular Weight:217.627
Hs Code.:

Synonyms:ethyl 6-amino-2-chloro-3-fluorobenzoate

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Chemical Property of ethyl 6-amino-2-chloro-3-fluorobenzoate

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Technology Process of ethyl 6-amino-2-chloro-3-fluorobenzoate

There total 3 articles about ethyl 6-amino-2-chloro-3-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1610927-38-2
ethyl 6-bromo-2-chloro-3-fluorobenzoate

: 153500-76-6
ethyl 6-amino-2-chloro-3-fluorobenzoate

Guidance literature:: With copper(I) oxide; ammonium hydroxide; In water; at 80 ℃; for 12h; Sealed tube;
DOI:10.1016/j.cclet.2014.03.021

Reference yield:

: 451-02-5
ethyl 3-fluorobenzoate

: 153500-76-6
ethyl 6-amino-2-chloro-3-fluorobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; palladium diacetate; sodium persulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 9 h / 80 °C

2: N-chloro-succinimide; palladium diacetate; sodium persulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 4 h / 80 °C

3: copper(I) oxide; ammonium hydroxide / water / 12 h / 80 °C / Sealed tube

With copper(I) oxide; ammonium hydroxide; sodium persulfate; N-chloro-succinimide; N-Bromosuccinimide; trifluorormethanesulfonic acid; palladium diacetate; In water; 1,2-dichloro-ethane;
DOI:10.1016/j.cclet.2014.03.021

Reference yield:

: 139911-28-7
ethyl 2-bromo-5-fluorobenzoate

: 153500-76-6
ethyl 6-amino-2-chloro-3-fluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide; palladium diacetate; sodium persulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 4 h / 80 °C

2: copper(I) oxide; ammonium hydroxide / water / 12 h / 80 °C / Sealed tube

With copper(I) oxide; ammonium hydroxide; sodium persulfate; N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate; In water; 1,2-dichloro-ethane;
DOI:10.1016/j.cclet.2014.03.021