2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

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Chemical Name:2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone
CAS No.:134970-23-3
Molecular Formula:C₆₄H₅₈O₉
Molecular Weight:971.159
Hs Code.:

2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

Synonyms:2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

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Chemical Property of 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

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Technology Process of 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

There total 4 articles about 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134970-21-1
8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

: 134970-23-3
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086

Reference yield:

: 134970-17-5
(2R,3R,4R,6R)-3,4-Bis-(biphenyl-4-ylmethoxy)-6-(1-methoxy-vinyl)-2-methyl-tetrahydro-pyran

: 134970-23-3
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086

Reference yield:

: 135004-20-5
C₇₄H₇₁N₃O₁₂

: 134970-23-3
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1021/ja00016a086