8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

Base Information

Chemical Name:8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde
CAS No.:134970-21-1
Molecular Formula:C₃₂H₂₉NO₃
Molecular Weight:475.587
Hs Code.:

Synonyms:8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

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Chemical Property of 8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

Chemical Property:

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Technology Process of 8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

There total 1 articles about 8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₅H₃₅N₃O₄

: 134970-21-1
8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 40 ℃; for 12h; Yield given;
DOI:10.1021/ja00016a086

Reference yield:

: 134970-21-1
8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

: 134970-22-2
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086

Reference yield:

: 134970-21-1
8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

: 134970-23-3
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-1,5-dihydroxy-anthraquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086