2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Base Information

Chemical Name:2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde
CAS No.:134970-22-2
Molecular Formula:C₆₆H₆₀O₇
Molecular Weight:965.198
Hs Code.:

2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Synonyms:2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

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Chemical Property of 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

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Technology Process of 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

There total 3 articles about 2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 135004-20-5
C₇₄H₇₁N₃O₁₂

: 134970-22-2
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 40 ℃; for 12h;
DOI:10.1021/ja00016a086

Reference yield:

: 134970-21-1
8-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-benzo[g]isoquinoline-9-carbaldehyde

: 134970-22-2
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086

Reference yield:

: 134970-17-5
(2R,3R,4R,6R)-3,4-Bis-(biphenyl-4-ylmethoxy)-6-(1-methoxy-vinyl)-2-methyl-tetrahydro-pyran

: 134970-22-2
2-[(R)-2-(Biphenyl-4-ylmethoxy)-4-hydroxy-2-methyl-butyl]-6-[(2R,4R,5R,6R)-4,5-bis-(biphenyl-4-ylmethoxy)-6-methyl-tetrahydro-pyran-2-yl]-anthracene-1,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) CaCO₃ / 1.) CH₃CN, 65 deg C, 10 h, 2.) MeOH, 10 deg C, 6 h

2: 79 percent / 3 N HCl / tetrahydrofuran / 12 h / 40 °C

With hydrogenchloride; calcium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00016a086