C₁₈H₁₅IN₂O

Base Information

Chemical Name:C₁₈H₁₅IN₂O
CAS No.:1314451-28-9
Molecular Formula:C₁₈H₁₅IN₂O
Molecular Weight:402.234
Hs Code.:

C<sub>18</sub>H<sub>15</sub>IN<sub>2</sub>O

Synonyms:C₁₈H₁₅IN₂O

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Chemical Property of C₁₈H₁₅IN₂O

Chemical Property:

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Technology Process of C₁₈H₁₅IN₂O

There total 7 articles about C₁₈H₁₅IN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1314451-10-9
2-(4-(4-methoxyphenyl)but-3-ynyl)-1H-benzo[d]imidazole

: 1314451-28-9
C₁₈H₁₅IN₂O

Guidance literature:: With iodine; sodium carbonate; silver nitrate; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/adsc.201100038

Reference yield:

: 6089-09-4
4-pentynoic acid

: 1314451-28-9
C₁₈H₁₅IN₂O

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 24 h / 20 °C

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine / 2 h / 20 °C

3: potassium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / methanol / 20 °C

5: acetic acid / 5 h / 90 °C / Inert atmosphere

6: iodine; sodium carbonate; silver nitrate / tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; sodium carbonate; silver nitrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; potassium hydroxide; In tetrahydrofuran; methanol; water; 2: Sonogashira coupling;
DOI:10.1002/adsc.201100038

Reference yield:

: 63093-41-4
ethyl 4-pentynoate

: 1314451-28-9
C₁₈H₁₅IN₂O

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine / 2 h / 20 °C

2: potassium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / methanol / 20 °C

4: acetic acid / 5 h / 90 °C / Inert atmosphere

5: iodine; sodium carbonate; silver nitrate / tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; sodium carbonate; silver nitrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; potassium hydroxide; In tetrahydrofuran; methanol; water; 1: Sonogashira coupling;
DOI:10.1002/adsc.201100038