3-Iodo-4-phenyl-1,2-dihydronaphthalene

Base Information

Chemical Name:3-Iodo-4-phenyl-1,2-dihydronaphthalene
CAS No.:117408-90-9
Molecular Formula:C16H13 I
Molecular Weight:332.184
Hs Code.:
DSSTox Substance ID:DTXSID40479079
Nikkaji Number:J2.181.451B
Wikidata:Q82312959
Mol file:117408-90-9.mol

Synonyms:3-Iodo-4-phenyl-1,2-dihydronaphthalene;117408-90-9;3-IODO-4-PHENYL-1,2-DIHYDRO-NAPHTHALENE;DTXSID40479079;AKOS015965715

Suppliers and Price of 3-Iodo-4-phenyl-1,2-dihydronaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-IODO-4-PHENYL-1,2-DIHYDRO-NAPHTHALENE 95.00%
5MG
$ 495.20

Total 2 raw suppliers

Chemical Property of 3-Iodo-4-phenyl-1,2-dihydronaphthalene

Chemical Property:

Vapor Pressure:7.63E-06mmHg at 25°C
Melting Point:80-81 °C
Refractive Index:1.691
Boiling Point:386.9°C at 760 mmHg
Flash Point:184.2°C
PSA：0.00000
Density:1.58g/cm³
LogP:4.82720
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:332.00620
Heavy Atom Count:17
Complexity:299

Purity/Quality:: 3-IODO-4-PHENYL-1,2-DIHYDRO-NAPHTHALENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=C(C2=CC=CC=C21)C3=CC=CC=C3)I

Technology Process of 3-Iodo-4-phenyl-1,2-dihydronaphthalene

There total 8 articles about 3-Iodo-4-phenyl-1,2-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 40164-53-2
1,4-diphenyl-1-butyne

: 117408-90-9
2-iodo-1-phenyl-3,4-dihydronaphthalene

Guidance literature:: With iodine; In water; at 20 ℃; for 2h;
DOI:10.1039/b500303b

Reference yield: 52.0%

: 123994-49-0
3,4-dihydro-1-naphthyl triflate

: 1078-58-6
diphenylzinc

: 4-iodo-3-phenyl-1,2-dihydronaphthalene

: 117408-90-9
2-iodo-1-phenyl-3,4-dihydronaphthalene

Guidance literature:: diphenylzinc; With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; di-n-butylzinc; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere; Schlenk technique; Sealed tube;

3,4-dihydro-1-naphthyl triflate; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere; Schlenk technique; Sealed tube;

With iodine; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/anie.202109482

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 117408-90-9
2-iodo-1-phenyl-3,4-dihydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium / diethyl ether / 0.33 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / benzene / 2 h / Reflux

3.1: iodine; silver trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C

With iodine; silver trifluoromethanesulfonate; lithium; toluene-4-sulfonic acid; In diethyl ether; acetonitrile; benzene;
DOI:10.1039/c0ob01107j