DL-m-FPhe-N-carboxyanhydride

Base Information

• Chemical Name: DL-m-FPhe-N-carboxyanhydride
• CAS No.: 87184-31-4
• Molecular Formula: C₁₀H₈FNO₃
• Molecular Weight: 209.177

Synonyms:DL-m-FPhe-N-carboxyanhydride

Chemical Property of DL-m-FPhe-N-carboxyanhydride

Chemical Property:

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Technology Process of DL-m-FPhe-N-carboxyanhydride

There total 1 articles about DL-m-FPhe-N-carboxyanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

phosgene (75-44-5) + 3-fluorophenylalanine (456-88-2,2629-54-1) → DL-m-FPhe-N-carboxyanhydride (87184-31-4)

Guidance literature:

In tetrahydrofuran; for 2h; Heating;

DOI:10.1021/jm00366a013

Reference yield:

L-alanin (56-41-7,25191-17-7,18875-37-1) + DL-m-FPhe-N-carboxyanhydride (87184-31-4) → D-m-FPhe-L-Ala (87184-21-2) + L-m-FPhe-L-Ala (87184-20-1)

Guidance literature:

With sodium hydroxide; sodium carbonate; In acetonitrile; at -10 ℃; for 3h;

DOI:10.1021/jm00366a013

upstream raw materials:

phosgene

3-fluorophenylalanine

Downstream raw materials:

D-m-FPhe-L-Ala

L-m-FPhe-L-Ala

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