C₄₇H₇₅N₅O₁₄

Base Information Edit

Chemical Name:C₄₇H₇₅N₅O₁₄
CAS No.:185461-57-8
Molecular Formula:C₄₇H₇₅N₅O₁₄
Molecular Weight:934.138
Hs Code.:
Mol file:185461-57-8.mol

C<sub>47</sub>H<sub>75</sub>N<sub>5</sub>O<sub>14</sub>

Synonyms:C₄₇H₇₅N₅O₁₄

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Chemical Property of C₄₇H₇₅N₅O₁₄ Edit

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Technology Process of C₄₇H₇₅N₅O₁₄

There total 13 articles about C₄₇H₇₅N₅O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 185461-56-7
Boc-Thr[Z-N(Me)-O(Me)-Tyr]-Ist-Hip-Leu-Pro-OBzl

: 185461-57-8
C₄₇H₇₅N₅O₁₄

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 3h; under 760 Torr; Ambient temperature;
DOI:10.1021/jo961932h

Reference yield:

: 15260-10-3
N-Boc-O-benzyl-L-threonine

: 185461-57-8
C₄₇H₇₅N₅O₁₄

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent Turnov_. / Li₂CO₃, 4 Angstroem molecular sieves / dimethylformamide / 18 h / Ambient temperature

2: 97 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr / Ambient temperature

3: 88 percent / DCC, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

4: 72 percent / aq. HF / acetonitrile / 7 h / -25 - -15 °C

5: 1-hydroxybenzotriazole, N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide, N,N-diisopropylethylamine / tetrahydrofuran / 4 h / -10 - -5 °C

6: 99 percent / H₂ / Pd/C / tetrahydrofuran / 3 h / 760 Torr / Ambient temperature

With dmap; 4 A molecular sieve; N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen fluoride; hydrogen; lithium carbonate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo961932h

Reference yield:

: 126587-71-1
Boc-threonine [(2-trimethylsilyl)ethoxy]methyl ester

: 185461-57-8
C₄₇H₇₅N₅O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / DCC, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

2: 72 percent / aq. HF / acetonitrile / 7 h / -25 - -15 °C

3: 1-hydroxybenzotriazole, N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide, N,N-diisopropylethylamine / tetrahydrofuran / 4 h / -10 - -5 °C

4: 99 percent / H₂ / Pd/C / tetrahydrofuran / 3 h / 760 Torr / Ambient temperature

With dmap; N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen fluoride; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo961932h