4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

Base Information

Chemical Name:4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol
CAS No.:945609-15-4
Molecular Formula:C₂₂H₃₂O₄
Molecular Weight:360.494
Hs Code.:

Synonyms:4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

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Chemical Property of 4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

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Technology Process of 4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

There total 4 articles about 4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 851341-17-8
acetic acid (2E,6E,10E)-12-(4-formyloxy-2-methoxy-phenoxy)-3,7,11-trimethyl-dodeca-2,6,10-trienyl ester

: 945609-15-4
4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

Guidance literature:: With methanol; potassium carbonate; for 2h;
DOI:10.1016/j.tet.2007.03.069

Reference yield:

: 93787-91-8
E,E,E-12-hydroxyfarnesyl acetate

: 945609-15-4
4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: 94 percent / potassium carbonate; methanol / 2 h

With methanol; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.tet.2007.03.069

Reference yield:

: 67431-17-8
4-hydroxy-3-methoxyphenyl formate

: 945609-15-4
4-[(2E,6E,10E)-12-hydroxy-2,6,10-trimethyl-dodeca-2,6,10-trienyloxy]-3-methoxy-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: 94 percent / potassium carbonate; methanol / 2 h

With methanol; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.tet.2007.03.069