tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

Base Information

Chemical Name:tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate
CAS No.:1333331-75-1
Molecular Formula:C₂₉H₂₈N₂O₄
Molecular Weight:468.552
Hs Code.:

Synonyms:tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

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Chemical Property of tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

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Technology Process of tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

There total 6 articles about tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333331-74-0
5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-carboxylic acid

: 75-65-0
tert-butyl alcohol

: 1333331-75-1
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

Guidance literature:: With diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; at 18 - 80 ℃; for 16h;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1333331-75-1
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; methanol / 4.5 h / Reflux

2: hydrogenchloride / water / 16 h / Reflux

3: manganese(IV) oxide / tetrahydrofuran / 3 h / Reflux

4: sodium chlorite / water; acetone / 3 h / 18 - 25 °C

5: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / 16 h / 18 - 80 °C

With hydrogenchloride; manganese(IV) oxide; sodium chlorite; diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; acetone; 5: Curtis Rearrangement;

Reference yield:

: 100-44-7
benzyl chloride

: 1333331-75-1
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; methanol / 4.5 h / Reflux

2: hydrogenchloride / water / 16 h / Reflux

3: manganese(IV) oxide / tetrahydrofuran / 3 h / Reflux

4: sodium chlorite / water; acetone / 3 h / 18 - 25 °C

5: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / 16 h / 18 - 80 °C

With hydrogenchloride; manganese(IV) oxide; sodium chlorite; diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; acetone; 5: Curtis Rearrangement;