tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

Base Information

Chemical Name:tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate
CAS No.:1333331-77-3
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

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Chemical Property of tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

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Technology Process of tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

There total 7 articles about tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333331-75-1
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]carbamate

: 74-88-4
methyl iodide

: 1333331-77-3
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 65 ℃; for 18h;

Reference yield:

: 100-44-7
benzyl chloride

: 1333331-77-3
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / water; methanol / 4.5 h / Reflux

2: hydrogenchloride / water / 16 h / Reflux

3: manganese(IV) oxide / tetrahydrofuran / 3 h / Reflux

4: sodium chlorite / water; acetone / 3 h / 18 - 25 °C

5: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / 16 h / 18 - 80 °C

6: caesium carbonate / N,N-dimethyl-formamide / 18 h / 65 °C

With hydrogenchloride; manganese(IV) oxide; sodium chlorite; diphenyl phosphoryl azide; caesium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone; 5: Curtis Rearrangement;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1333331-77-3
tert-butyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridine-2-yl]methylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / water; methanol / 4.5 h / Reflux

2: hydrogenchloride / water / 16 h / Reflux

3: manganese(IV) oxide / tetrahydrofuran / 3 h / Reflux

4: sodium chlorite / water; acetone / 3 h / 18 - 25 °C

5: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / 16 h / 18 - 80 °C

6: caesium carbonate / N,N-dimethyl-formamide / 18 h / 65 °C

With hydrogenchloride; manganese(IV) oxide; sodium chlorite; diphenyl phosphoryl azide; caesium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone; 5: Curtis Rearrangement;