4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

Base Information

Chemical Name:4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate
CAS No.:188562-93-8
Molecular Formula:C₁₉H₂₄F₃NO₅S
Molecular Weight:435.464
Hs Code.:

Synonyms:4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

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Chemical Property of 4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

There total 5 articles about 4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 188562-93-8
4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 4 Angstroem molecular sieves, 2.) NaBH₄ / 1.) CH₂Cl₂, 4 h, 2.) MeOH, 0 deg C, 4 h.

2: 88 percent / 3 N HCl / tetrahydrofuran / 10 h / Heating

3: 85 percent / Et₃N / methanol / 2 h / 60 °C

4: 1.) LiHMDS / 1.) THF, -78 deg C, 2 h, 2.) room temperature, 5 h.

With hydrogenchloride; sodium tetrahydroborate; 4 A molecular sieve; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(96)01051-4

Reference yield:

: 131511-13-2
4-(N-benzylamino)cyclohexanone ethylene acetal

: 188562-93-8
4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 3 N HCl / tetrahydrofuran / 10 h / Heating

2: 85 percent / Et₃N / methanol / 2 h / 60 °C

3: 1.) LiHMDS / 1.) THF, -78 deg C, 2 h, 2.) room temperature, 5 h.

With hydrogenchloride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(96)01051-4

Reference yield:

: 142009-99-2
4-(benzylamino)cyclohexane-1-one

: 188562-93-8
4-[N-benzyl-N-(tert-butoxycarbonyl)amino]cyclohex-1-en-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / methanol / 2 h / 60 °C

2: 1.) LiHMDS / 1.) THF, -78 deg C, 2 h, 2.) room temperature, 5 h.

With triethylamine; lithium hexamethyldisilazane; In methanol;
DOI:10.1016/S0040-4020(96)01051-4