2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

Base Information

Chemical Name:2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine
CAS No.:96444-52-9
Molecular Formula:C₁₈H₁₉N₃OS
Molecular Weight:325.434
Hs Code.:

Synonyms:2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

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Chemical Property of 2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

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Technology Process of 2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

There total 6 articles about 2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 96428-63-6
2-methyl-3-<(methylcarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

: 96444-52-9
2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

Guidance literature:: With diphosphorus pentasulfide; In 1,2-dimethoxyethane; at 70 ℃; for 8h;
DOI:10.1021/jm00145a006

Reference yield:

: 927-56-0
levulinonitrile

: 96444-52-9
2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 45 percent / etheral hydrogen chloride, sulfuryl chloride / ethanol / 2.75 h / 20 °C

2: triethylamine / ethanol / 24 h / Heating

3: 34 percent / sodium hydroxide / H₂O; methanol / 3 h / Heating

4: 30 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂

5: 38 percent / phosphorus pentasulfide / 1,2-dimethoxy-ethane / 8 h / 70 °C

With hydrogenchloride; diphosphorus pentasulfide; sodium hydroxide; sulfuryl dichloride; triethylamine; dicyclohexyl-carbodiimide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water;
DOI:10.1021/jm00145a006

Reference yield:

: 76081-98-6
3-(cyanomethyl)-2-methyl-8-(phenylmethoxy)imidazo[1,2-a]pyridine

: 96444-52-9
2-methyl-3-<(methylthiocarbamoyl)methyl>-8-(phenylmethoxy)imidazo<1,2-a>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / sodium hydroxide / H₂O; methanol / 3 h / Heating

2: 30 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂

3: 38 percent / phosphorus pentasulfide / 1,2-dimethoxy-ethane / 8 h / 70 °C

With diphosphorus pentasulfide; sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/jm00145a006