N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

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Chemical Name:N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine
CAS No.:330938-08-4
Molecular Formula:C₂₃H₃₃NO₂
Molecular Weight:355.521
Hs Code.:

Synonyms:N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

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Chemical Property of N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

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Technology Process of N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

There total 4 articles about N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 224967-65-1
1-hydroxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

: 74-88-4
methyl iodide

: 330938-08-4
N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: 1-hydroxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; for 7h; Further stages.; Heating;
DOI:10.1021/jo001190z

Reference yield:

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 330938-08-4
N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 64 percent / Cu; Cu(OTf)2; 4,4-di-tert-butyl-2,2'-bipyridyl / benzene / 12 h / 65 - 70 °C

2.1: 83 percent / TBAF*3H₂O / tetrahydrofuran / 14 h / 20 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

3.2: 62 percent / tetrahydrofuran / 7 h / Heating

With 4,4-di-tert-butyl-2,2-bipyridine; tetrabutyl ammonium fluoride; copper(II) bis(trifluoromethanesulfonate); copper; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jo001190z

Reference yield:

: 270901-81-0
N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

: 330938-08-4
N-[1,1-dimethylethyl-1-(methoxy)]-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 64 percent / Cu; Cu(OTf)2; 4,4-di-tert-butyl-2,2'-bipyridyl / benzene / 12 h / 65 - 70 °C

2.1: 83 percent / TBAF*3H₂O / tetrahydrofuran / 14 h / 20 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

3.2: 62 percent / tetrahydrofuran / 7 h / Heating

With 4,4-di-tert-butyl-2,2-bipyridine; tetrabutyl ammonium fluoride; copper(II) bis(trifluoromethanesulfonate); copper; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jo001190z