N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

Base Information

Chemical Name:N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl
CAS No.:270901-81-0
Molecular Formula:C₂₀H₃₆NO₂Si
Molecular Weight:350.597
Hs Code.:

Synonyms:N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

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Chemical Property of N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

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Technology Process of N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

There total 4 articles about N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 393110-72-0
N-[2-(tert-butyl-dimethyl-silanyloxy)-1,1-dimethyl-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

: 270901-81-0
N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

Guidance literature:: With ammonium hydroxide; copper diacetate; oxygen; In methanol;
DOI:10.1021/jo061194p

Reference yield:

: 293328-26-4
C₁₇H₂₉NO₂Si

: 270901-81-0
N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / tetrahydrofuran

2: 72 percent / O₂; Cu(OAc)2; NH₄OH / methanol

With ammonium hydroxide; copper diacetate; oxygen; In tetrahydrofuran; methanol;
DOI:10.1021/jo061194p

Reference yield:

: 55277-95-7
N-benzylidene-1-hydroxy-2-methyl-2-propanamine N-oxide

: 270901-81-0
N-(1,1-dimethyl-2-[tert-butyldimethylsilanyloxy]propyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Et₃N; DMAP / CH₂Cl₂

2: 69 percent / tetrahydrofuran

3: 72 percent / O₂; Cu(OAc)2; NH₄OH / methanol

With dmap; ammonium hydroxide; copper diacetate; oxygen; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo061194p