Technology Process of C20H33BN2O6
There total 1 articles about C20H33BN2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-formylphenylboronic acid,; N-Boc-1,3-diaminopropane;
In
ethanol;
at 20 ℃;
for 2h;
Inert atmosphere;
With
sodium tetrahydroborate; ethanol;
In
toluene;
at 0 - 20 ℃;
for 3.33333h;
di-tert-butyl dicarbonate;
With
potassium carbonate;
In
tetrahydrofuran; water;
at 20 ℃;
for 23h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate / water; methanol / 5.5 h / 20 °C
2: pyridine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
With
pyridine;
N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate;
In
tetrahydrofuran; methanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate / water; methanol / 5.5 h / 20 °C
2.1: pyridine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
3.1: triethylamine / tetrakis(triphenylphosphine) palladium(0); copper(l) iodide / N,N-dimethyl-formamide / 14.25 h / 22 - 85 °C / Inert atmosphere; Sealed vessel
3.2: 3 h / 90 °C / Sealed vessel
With
pyridine; triethylamine;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
