E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

Base Information

Chemical Name:E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime
CAS No.:169153-13-3
Molecular Formula:C₁₁H₁₂N₂O₄
Molecular Weight:236.227
Hs Code.:

Synonyms:E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

Suppliers and Price of E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Technology Process of E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

There total 14 articles about E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₁₁H₁₂N₂O₄

: 169153-14-4
(E)-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxyphenyl)-methanone O-methyloxime

: 169153-13-3
E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

Guidance literature:: C₁₁H₁₂N₂O₄; With hydrogenchloride; In acetic acid butyl ester; at 0 - 5 ℃; for 4h; Acidic conditions;

With sodium hydroxide; In acetic acid butyl ester; water; at 0 - 5 ℃; pH=3 - 9; Product distribution / selectivity; Alkaline conditions;

Reference yield: 50.35%

: Z-(5,6-Dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone oxime

: 77-78-1
dimethyl sulfate

: 169153-13-3
E-(5,6-dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone O-methyl-oxime

Guidance literature:: Z-(5,6-Dihydro-[1,4,2]dioxazin-3-yl)-(2-hydroxy-phenyl)-methanone oxime; With sodium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;

dimethyl sulfate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 16h;