N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Base Information

• Chemical Name: N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine
• CAS No.: 1424338-86-2
• Molecular Formula: C₆₂H₇₄N₄O₁₄Si₂
• Molecular Weight: 1155.46

Synonyms:N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Chemical Property of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Chemical Property:

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Technology Process of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

There total 1 articles about N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine (1424338-84-0) + acetic anhydride (108-24-7) → N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine (1424338-86-2)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo402665d

Reference yield: 78.0%

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine (1424338-86-2) → N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine (1424338-88-4)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield:

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine (1424338-86-2) → C52H58N4O10Si2 (1582314-27-9)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo402665d

upstream raw materials:

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

acetic anhydride

Downstream raw materials:

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

5-(3′-deoxy-3′-oxo-2′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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