N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Chemical Name:N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine
CAS No.:1424338-92-0
Molecular Formula:C₄₉H₅₀N₄O₁₄
Molecular Weight:918.954
Hs Code.:

Synonyms:N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Chemical Property of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Technology Process of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

There total 3 articles about N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1424338-89-5
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 1424338-92-0
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: With Dess-Martin periodane; at 20 ℃; for 1h;

Reference yield:

: 1424338-88-4
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 1424338-92-0
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: Dess-Martin periodane / 1 h / 20 °C

With Dess-Martin periodane; triethylamine; In dichloromethane;

Reference yield:

: 1424338-86-2
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 1424338-92-0
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-trityl-3′-deoxy-3′-O-acetyl-β-D-ribofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 48 h / 20 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

3: Dess-Martin periodane / 1 h / 20 °C

With Dess-Martin periodane; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; dichloromethane;