N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Chemical Name:N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine
CAS No.:1424338-89-5
Molecular Formula:C₄₉H₅₂N₄O₁₄
Molecular Weight:920.97
Hs Code.:

Synonyms:N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Chemical Property of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

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Technology Process of N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

There total 2 articles about N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1424338-88-4
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 76-83-5
trityl chloride

: 1424338-89-5
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1424338-86-2
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-[3′,5′-di-O-(tert-butyldiphenylsilyl)-2′-O-acetyl-β-D-xylofuranosyl]-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

: 1424338-89-5
N,N-bis[(1,1-dimethylethoxy)carbonyl]-5-(5′-O-trityl-2′-O-acetyl-β-D-xylofuranosyl)-3-nitro-6-[2-(4-nitrophenyl)ethoxy]-2-pyridinamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 48 h / 20 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

With triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; dichloromethane;