3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Base Information

Chemical Name:3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester
CAS No.:117085-35-5
Molecular Formula:C₁₇H₂₀O₅
Molecular Weight:304.343
Hs Code.:

Synonyms:3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Suppliers and Price of 3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

There total 3 articles about 3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 105346-32-5
ethyl 3-(4-hydroxy-5-oxo-3-phenyl-2,5-dihydro-2-furyl)propionate

: 117085-35-5
3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 4h; Ambient temperature;
DOI:10.1248/cpb.36.1404

Reference yield:

: 156-06-9
2-oxo-3-(phenyl)propionic acid

: 117085-35-5
3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / DBU / dimethylformamide / 2.5 h / 0 °C

2: 72 percent / DBU / dimethylformamide / 2.5 h

3: 81 percent / K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.1404

Reference yield:

: 6362-58-9
methyl phenylpyruvate

: 117085-35-5
3-(4-Ethoxy-5-oxo-3-phenyl-2,5-dihydro-furan-2-yl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / DBU / dimethylformamide / 2.5 h

2: 81 percent / K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.1404