2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine
CAS No.:1609496-77-6
Molecular Formula:C₁₆H₂₂BrNOS
Molecular Weight:356.327
Hs Code.:

Synonyms:2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

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Technology Process of 2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

There total 4 articles about 2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1609496-76-5
4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenol

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 1609496-77-6
2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: With sodium hydroxide; In toluene; at 120 ℃; for 8h;
DOI:10.1021/ol501165h

Reference yield:

: 19614-12-1
2-bromo-5-methoxybenzyl bromide

: 1609496-77-6
2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: acetone / 20 °C

2: boron tribromide / dichloromethane / 12 h / 0 - 20 °C

3: potassium hydroxide / ethanol / 0.5 h / 20 °C

4: sodium hydroxide / toluene / 8 h / 120 °C

With boron tribromide; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; acetone; toluene;
DOI:10.1021/ol501165h

Reference yield:

: 1609496-74-3
S-(2-bromo-5-methoxybenzyl)ethanethioate

: 1609496-77-6
2-(4-bromo-3-((pent-2-yn-1-ylthio)methyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / 12 h / 0 - 20 °C

2: potassium hydroxide / ethanol / 0.5 h / 20 °C

3: sodium hydroxide / toluene / 8 h / 120 °C

With boron tribromide; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; toluene;
DOI:10.1021/ol501165h