1-aminopyridinium mesitylenesulphonate

Base Information

• Chemical Name: 1-aminopyridinium mesitylenesulphonate
• CAS No.: 39996-41-3
• Molecular Formula: C₅H₇N₂*C₉H₁₁O₃S
• Molecular Weight: 294.375
• Mol file: 39996-41-3.mol

Synonyms:1-aminopyridinium mesitylenesulphonate

Chemical Property of 1-aminopyridinium mesitylenesulphonate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-aminopyridinium mesitylenesulphonate

There total 2 articles about 1-aminopyridinium mesitylenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

→ 1-aminopyridinium mesitylenesulphonate (39996-41-3)

Guidance literature:

Reference yield:

pyridine (110-86-1) + mesitylenesulfonylhydroxylamine (36016-40-7) → 1-aminopyridinium mesitylenesulphonate (39996-41-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.166667h;

DOI:10.1002/jhet.5570440622

Reference yield: 88.0%

methyl dithiobenzoate (2168-78-7) + 1-aminopyridinium mesitylenesulphonate (39996-41-3) → pyridinium 1-[(phenyl)thiocarbonyl]aminide (87290-01-5)

Guidance literature:

With potassium carbonate; In ethanol; for 2.5h; Ambient temperature;

DOI:10.1246/bcsj.56.1561

upstream raw materials:

pyridine

mesitylenesulfonylhydroxylamine

Downstream raw materials:

1-Acetylpyrazolo<1,5-a>pyridine

pyridinium 1-[(phenyl)thiocarbonyl]aminide

1-pyridinio(p-methoxybenzenethiocarbonyl)amidate

3-benzoyl-2-methylthioimidazo<1,2-a>pyridine

Refernces

• 1、 -. "Heteroaryl imidazolone derivatives as jak inhibitors". Page/Page column 105-106. . Retrieved 2012/01/06.
• 2、 Johnston, Karen A.,Allcock, Robert W.,Jiang, Zhong,Collier, Ian D.,Blakli, Haakon,Rosair, Georgina M.,Bailey, Patrick D.,Morgan, Keith M.,Kohno, Yasushi,Adams, David R.. "Concise routes to pyrazolo[1,5-a]pyridin-3-yl pyridazin-3-ones". . p. 175 - 186. Retrieved 2008/09/20.