1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

Base Information

Chemical Name:1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine
CAS No.:167710-59-0
Molecular Formula:C₂₁H₃₃ClN₂O₂
Molecular Weight:380.958
Hs Code.:

Synonyms:1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

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Chemical Property of 1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

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Technology Process of 1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

There total 3 articles about 1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 882-09-7
Clofibric acid

: 167649-35-6
β,β-dimethyl-N,N-dimethyl-4-piperidineethanamine

: 167710-59-0
1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

Guidance literature:: Clofibric acid; With dicyclohexyl-carbodiimide; In chloroform; at 0 ℃; for 0.5h;

β,β-dimethyl-N,N-dimethyl-4-piperidineethanamine; In chloroform; for 24h;
DOI:10.1248/cpb.50.316

Reference yield:

: 696-30-0
4-s-propylpyridine

: 167710-59-0
1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 42 percent / aq. AcOH / 72 h / Heating

2.1: 100 percent / H₂; AcOH / PtO₂ / 7 h / 80 °C / 51714.8 Torr

3.1: 1,3-dicyclohexylcarbodiimide / CHCl₃ / 0.5 h / 0 °C

3.2: 60 percent / CHCl₃ / 24 h

With hydrogen; acetic acid; dicyclohexyl-carbodiimide; platinum(IV) oxide; In chloroform; 1.1: Mannich reaction;
DOI:10.1248/cpb.50.316

Reference yield:

: 167649-34-5
β,β-dimethyl-N,N-dimethyl-4-pyridineethanamine

: 167710-59-0
1-[2-(4-chlorophenoxy)-2-methyl-1-oxopropyl]-β,β,N,N-tetramethyl-4-piperidineethaneamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / H₂; AcOH / PtO₂ / 7 h / 80 °C / 51714.8 Torr

2.1: 1,3-dicyclohexylcarbodiimide / CHCl₃ / 0.5 h / 0 °C

2.2: 60 percent / CHCl₃ / 24 h

With hydrogen; acetic acid; dicyclohexyl-carbodiimide; platinum(IV) oxide; In chloroform;
DOI:10.1248/cpb.50.316