3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Base Information

Chemical Name:3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione
CAS No.:1415214-11-7
Molecular Formula:C₂₃H₁₉N₃O₅
Molecular Weight:417.421
Hs Code.:

Synonyms:3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Chemical Property of 3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Technology Process of 3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

There total 8 articles about 3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3645-45-2
phthaloyldihydrazine

: 126-81-8
dimedone

: 552-89-6
2-nitro-benzaldehyde

: 1415214-11-7
3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With phosphotungstic acid supported on 1,4-phenylenediamine-modified silica-coated manganese ferrite with H₃PW₁₂O₄₀ nanoparticles; In neat (no solvent); at 80 ℃; for 0.333333h; Solvent;
DOI:10.1016/j.poly.2019.01.065

Reference yield: 93.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 3471-13-4
dimedone

: 552-89-6
2-nitro-benzaldehyde

: 1415214-11-7
3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With SBA-15 sulfonic acid mesoporous silicas; In acetonitrile; at 45 ℃; for 0.333333h; Irradiation; Green chemistry;
DOI:10.1016/j.molcata.2013.03.017

Reference yield: 93.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 126-81-8
dimedone

: 552-89-6
2-nitro-benzaldehyde

: 1415214-11-7
3,3-dimethyl-13-(2-nitrophenyl)-2,3,4,6,11,13-hexahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With nano (SO₃H functionalized mesoporous silica); In neat (no solvent); at 110 ℃; for 0.333333h; Sealed tube; Green chemistry;
DOI:10.1039/c5nj01733e