2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

Base Information

Chemical Name:2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate
CAS No.:1250395-63-1
Molecular Formula:C₂₉H₄₇NO₅Si
Molecular Weight:517.781
Hs Code.:

Synonyms:2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

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Chemical Property of 2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

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Technology Process of 2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

There total 1 articles about 2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40630-84-0
allyl bromoacetate

: 1250395-62-0
(3S,6R,4Z)-6-[(tert-butyldimethylsilyloxy)methyl]-3-(4-methoxyphenylmethoxy)-4-methyl-4-octenenitrile

: 1250395-63-1
2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

Guidance literature:: With bis(cyclopentadienyl)titanium dichloride; zinc; In tetrahydrofuran; at 60 ℃;
DOI:10.1002/anie.201002293

Reference yield:

: 1250395-63-1
2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate

: 1133769-93-3
(4S,7R)(5Z)-4-[(4-methoxyphenyl)methoxy]-5-methyl-7-[(1,1,2,2-tetramethyl-1-silapropoxy)methyl]non-5-en-2-one

: 1250395-70-0
C₁₉H₂₈O₄

Guidance literature:: 2-propenyl (2Z,5S,8R,6Z)-3-amino-8-[(tert-butyldimethylsilyloxy)methyl]-5-(4-methoxyphenylmethoxy)-6-methyl-2,6-decadienoate; With water; In tetrahydrofuran; isopropyl alcohol; for 22h; pH=3; aq. phosphate buffer;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/anie.201002293