(2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

Base Information

Chemical Name:(2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine
CAS No.:1101862-56-9
Molecular Formula:C₁₉H₂₂BrNO₃
Molecular Weight:392.293
Hs Code.:

Synonyms:(2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

Suppliers and Price of (2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

There total 1 articles about (2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 90-82-4,7009-81-6,90-83-5,6912-63-6
pseudoephedrine

: 1101862-56-9
(2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

Guidance literature:: With acetic acid; In toluene; for 20h; Reflux;
DOI:10.1021/ol8026208

Reference yield:

: 181517-76-0
3-(3',4'-methylenedioxyphenyl)-(E)-propenoic acid tert-butyl ester

: 1101862-56-9
(2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine

: 106-95-6
allyl bromide

: C₃₆H₄₃NO₇

Guidance literature:: (2S,4S,5S)-2-(2-bromo-4,5-dimethoxyphenyl)-3,4-dimethyl-5-phenyloxazolidine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

3-(3',4'-methylenedioxyphenyl)-(E)-propenoic acid tert-butyl ester; allyl bromide; enantioselective reaction; Further stages;
DOI:10.1021/ol8026208