N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide

Base Information

• Chemical Name: N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide
• CAS No.: 910464-81-2
• Molecular Formula: C₃₀H₁₉NO₅
• Molecular Weight: 473.485
• Mol file: 910464-81-2.mol

Synonyms:N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide

Chemical Property of N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide

There total 7 articles about N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cyclohexyl-3,4-peryleneimide di-9,10-perylenedicarboxylic acid dihexyl ester → N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide (910464-81-2)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 90 ℃; for 4h;

Reference yield:

N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide (41572-86-5) → N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide (910464-81-2)

Guidance literature:

N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide; With potassium hydroxide; In water; isopropyl alcohol; at 85 ℃; for 3h;

With acetic acid; In water; isopropyl alcohol; at 20 ℃; for 0.25h;

DOI:10.1002/anie.201507186

Reference yield:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → N-(cyclohexyl)-3,4,9,10-perylenetetracarboxylic acid-3,4-anhydride-9,10-imide (910464-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 15 h / 140 °C

2.1: potassium hydroxide / water; isopropyl alcohol / 3 h / 85 °C

2.2: 0.25 h / 20 °C

With potassium hydroxide; In water; isopropyl alcohol;

DOI:10.1002/anie.201507186

upstream raw materials:

cyclohexylamine

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide

Downstream raw materials:

N-cyclohexyl-N'-dodecyl-perylene-3,4,9,10-tetracarboxylic diimide