2-fluorophenyl isopropylcarbamate

Base Information

Chemical Name:2-fluorophenyl isopropylcarbamate
CAS No.:199585-08-5
Molecular Formula:C₁₀H₁₂FNO₂
Molecular Weight:197.209
Hs Code.:

Synonyms:2-fluorophenyl isopropylcarbamate

Suppliers and Price of 2-fluorophenyl isopropylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-fluorophenyl isopropylcarbamate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2-fluorophenyl isopropylcarbamate

There total 1 articles about 2-fluorophenyl isopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 367-12-4
2-fluorophenol

: 1795-48-8
Isopropyl isocyanate

: 199585-08-5
2-fluorophenyl isopropylcarbamate

Guidance literature:: DOI:10.1055/s-2006-926462

Reference yield: 40.0%

: 199585-08-5
2-fluorophenyl isopropylcarbamate

: 6138-90-5
trans-geranyl bromide

: (E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-6-fluorophenyl isopropylcarbamate

Guidance literature:: 2-fluorophenyl isopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 25 ℃; for 0.5h;

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 1h;

trans-geranyl bromide; In tetrahydrofuran; hexane; at -78 ℃; for 3h;
DOI:10.1055/s-0039-1690111

Reference yield: 17.0%

: 199585-08-5
2-fluorophenyl isopropylcarbamate

: 6138-90-5
trans-geranyl bromide

: (E)-4-chloro-2-(3,7-dimethylocta-2,6-dien-1-yl)-6-fluorophenyl isopropylcarbamate

Guidance literature:: 2-fluorophenyl isopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 25 ℃; for 0.5h;

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 1h;

trans-geranyl bromide; In tetrahydrofuran; hexane; at -78 ℃; for 3h;
DOI:10.1055/s-0039-1690111