p-methoxybenzenetellurinic acid anhydride

Base Information

• Chemical Name: p-methoxybenzenetellurinic acid anhydride
• CAS No.: 97977-87-2
• Molecular Formula: C₁₄H₁₄O₅Te₂
• Molecular Weight: 517.462
• Mol file: 97977-87-2.mol

Synonyms:p-methoxybenzenetellurinic acid anhydride

Chemical Property of p-methoxybenzenetellurinic acid anhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-methoxybenzenetellurinic acid anhydride

There total 3 articles about p-methoxybenzenetellurinic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

[bis(acetoxy)iodo]benzene (3240-34-4) + bis(4-methoxyphenyl)ditelluride (35684-37-8) → p-methoxybenzenetellurinic acid anhydride (97977-87-2)

Guidance literature:

With sodium hydroxide; In dichloromethane; Ambient temperature;

DOI:10.1080/00397919508015845

Reference yield: 92.0%

p-methoxyphenyltellurium trichloride (36309-68-9) → p-methoxybenzenetellurinic acid anhydride (97977-87-2)

Guidance literature:

In tetrahydrofuran; sodium hydroxide; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90612-X

Reference yield:

C12H14Cl2O3Te (122182-98-3) → p-methoxybenzenetellurinic acid anhydride (97977-87-2)

Guidance literature:

With water; sodium carbonate;

upstream raw materials:

p-methoxyphenyltellurium trichloride

C₁₂H₁₄Cl₂O₃Te

[bis(acetoxy)iodo]benzene

bis(4-methoxyphenyl)ditelluride

Downstream raw materials:

2-<<(p-methoxyphenyl)telluro>methyl>-1-oxaspiro<5.5>undecane

1-<2-acetoxy-3-<(p-methoxyphenyl)telluro>propyl>cyclohexyl acetate

C₂₂H₂₆O₇Te

2-<<(p-methoxyphenyl)telluro>methyl>tetrahydropyran

Refernces

• 1、 Khandelwal, Bishan L.,Singh, Ajai K.,Bhandari, Narendra S.. "REACTIONS OF ACETYLACETONE WITH ORGANOTELLURIUM (IV) CHLORIDES-C1 BONDED ACETYLACETONATES OF TELLURIUM(IV)". . p. 157 - 166. Retrieved 2007/10/02.