Technology Process of C27H42O5Si2
There total 5 articles about C27H42O5Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / TPAP; NMO; MS 4A / CH2Cl2
2: H2O; Dowex 50W-X8 / methanol / 50 °C
3: Et3N / CH2Cl2
With
N-methyl-2-indolinone; tetrapropylammonium perruthennate; Dowex 50W-X8; water; triethylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.tetlet.2007.06.134
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2O; Dowex 50W-X8 / methanol / 50 °C
2: Et3N / CH2Cl2
With
Dowex 50W-X8; water; triethylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.tetlet.2007.06.134
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 53 percent / NaH / dimethylformamide
2.1: n-BuLi; TMEDA / tetrahydrofuran
2.2: 77 percent / tetrahydrofuran
3.1: 99 percent / TPAP; NMO; MS 4A / CH2Cl2
4.1: H2O; Dowex 50W-X8 / methanol / 50 °C
5.1: Et3N / CH2Cl2
With
n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; N,N,N,N,-tetramethylethylenediamine; Dowex 50W-X8; water; sodium hydride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.06.134