2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

Base Information

Chemical Name:2,6-dinitro-4-trifluoromethylsulfonylphenyl azide
CAS No.:107607-41-0
Molecular Formula:C₇H₂F₃N₅O₆S
Molecular Weight:341.184
Hs Code.:

Synonyms:2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

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Technology Process of 2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

There total 2 articles about 2,6-dinitro-4-trifluoromethylsulfonylphenyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 19822-34-5
2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

: 107607-41-0
2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

Guidance literature:: With sodium azide; In methanol; water; acetone; for 0.25h; in the dark;;

Reference yield:

: 19822-29-8
2,6-dinitro-4-((trifluoromethyl)sulfonyl)anisole

: 107607-41-0
2,6-dinitro-4-trifluoromethylsulfonylphenyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine hydrochloride; 2.) POCl₃ / 1.) 115-120 deg C; 2.) reflux for 0.5 h.

2: 95 percent / sodium azide / acetone; methanol; H₂O / 0.25 h / in the dark;

With sodium azide; pyridine hydrochloride; trichlorophosphate; In methanol; water; acetone;